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The inclusion of softeners (20 g/l), namely, Siligen VN (silicon based), Basosoft SWK (cationic), or Leomin NI (nonionic), in a dimethyloldihydroxy ethylene urea (DMDHEU, 50 g/l) finishing formulation of 65/35 cotton/polyester blended fabric, enhances the resiliency of the fabric, which is expressed as the dry wrinkle recovery angle (WRA). The fabric acquires the ability to keep a rose oil fragrance upon storage up to 3 months. Improving the WRA and acquiring the ability to keep the fragrance can be descendingly arranged as follows: Siligen VN>Basosoft SWK>Leomin NI. Increasing the Siligen VN concentration (0-30 g/l) in the finishing formulation is accompanied by a small increase in the WRA, and a noticeable enhancement in the ability to keep the rose oil fragrance upon storage. By increasing the rose oil concentration (100-300 g/l) in a perfumed bath of cross-linked/Siligen VN, the softened fabric is accompanied by a slight drop in the WRA, and a decreasing ability to keep the fragrance up to 3 months.

However, the extent of the fragrance is higher at higher rose oil concentrations, regardless of the storage time. The ability of the fabric to keep the fragrance can be attributed to solubilization and/or encapsulation of the perfume in the oleophilic segments of the softener, and its slow release with time, so that the smell can be sensed. This ability decreases after increasing the storage time up to 3 months, and depending on the type of perfume oil used, is descendingly arranged as follows: jasmine oil > rose oil > sandal oil.

Three different thermo-sensitive microgels obtained by the copolymerisation of vinylcaprolactam) (VCL) and various monomers (vinylimidazole(VIm), acetoacetoxyethyl methacrylate (AAEM) and itaconic acid(IA)) are used to coat different fibre surfaces. Two different pHs and two different temperatures, 25°C and 50°C respectively are chosen for the deposition of the microgels. The scanning electron microscopy of the treated fibre shows good distribution of the particles onto the fibres especially at increasing temperatures. The gloss index for the treated fibres has been measured, and showed that it may be controlled for all of the fibres with the treatment parameters (pH and temperature) and the microgel structure.

Functionalized polyethylenimine–dye (FPEI) is prepared by mixing branched polyethyleneimine (PEI), in which its primary amine groups are modified at different ratios with a quaternary ammonium coupler (QI), and reactive dyestuff (RD) (QI/RD = 0/100, 20/80, 40/60, 60/40 and 80/20 mole/mole %). The deposition of FPEI from an aqueous solution onto the surface of cotton and wool fibres is studied. The adsorption of a charged polymer from an aqueous medium by cotton and wool fibres is investigated at different pH values, and the uptake of colour on fibres is measured by Datacolor and UVVIS spectrophotometers.

The study of the kinetics of adsorption shows that pseudo-first-order kinetics provide the best correlation of the experimental data. The equilibrium data indicate that the deposition process onto both cotton and wool follows the Langmuir isotherm. In terms of colour strength (K/S value) the coated fibres compare well with those dyed with a commercial dyestuff, C.I. Basic Red 51, which suggests that the coating is a good alternative to classical dyeing.

Condensates of stearic (St), palmitic (Pa) or myristic (My) acids with polyethylene glycols (PEG) 300, 400, 600, 2000 or 6000, are utilized as emulsifiers for kerosene ∓ in ∓ water pigment printing pastes. Pastes based on condensates of PEG 300 or 400 are unstable while the others are stable. Rheology of stable pastes, aside from those based on a commercial emulsifier, are of a non ∓ Newtonian, shear thinning ∓ thixotropic flow. The order of the flow properties of pastes enhanced are found. Cotton pigment prints using the nine pastes are sharp and of comparable handle, colour strength and color fastness to those based on a paste of either a commercial emulsifier or synthetic thickener (except for Pa∓6000). The pigment prints of 65/35 cotton/polyester are sharp only upon using pastes of commercial emulsifier, synthetic thickener, St∓600, St∓2000, St∓6000 and My∓2000. After 7 days of storing, all pastes are stable with increased apparent viscosities and induced color strength on both cotton and blended fabrics.

Optimal conditions for condensation of equimolar ratios of stearic acid (St) and polyethylene glycol (PEG) 400, i.e. 180°C, 8hrs and H₂SO₄, 4g/kg (reactants mixture), were utilized to condensate the equimolar ratio of stearic (St), palmitic (Pa) or myristic (My) acid with PEG 300, 400, 600, 2000 or 6000. Each of the fifteen condensates was formed by total conversion (83.5 to 84.1 %). Monoester–diester ratios of the condensates ranged from 4:1 to 49:1. FT – IR spectroscopy and hydrophilic lipohilic balances (HLB) of the condensates were also examined. The condensates had softening and hydrophilic properties of cotton fabric with no yellowing at concentrations of 30 and 50g/l in the presence or absence of DMDHEU (50g/l). The presence of DMDHEU improved the fabric resiliency.

However, the softening and hydrophilic properties of the fabric were inferior in the presence of DMDHEU rather than the absence. In comparison with a commercial softener, PEG 2000- or 6000-based condensates were higher in fabric wettability and pliability but lower in smoothness. Regarding CRA, only My-2000 was comparable to that of the commercial softener in terms of effect.

This study aims to evaluate the thermal performance of phase change materials (PCMs) microcapsules (MCs) attached using SiO₂ microspheres and investigate the thermal regulation effect on the coated denim fabric.

The PCM microcapsule was prepared by in situ polymerization using a mixture of solid paraffin and butyl stearate as core material (CM) and methyl methacrylate as a monomer. The SiO₂ microparticles were attached to the outer layer of the membrane to enhance the thermal performance of MCs. The morphology, chemical structure, latent heat storage and thermal resistance of MCs were characterized. PCM MCs were coated on the denim fabric and thermo-gravimetric analysis was conducted; thermal insulation and thermal infrared imaging performance of the coated fabrics were also investigated.

The diameters of SiO₂ particles and PCMs MCs were 300-500 nm and 1 μm, respectively. SiO₂ was wrapped on single-wall PCMs MCs with the mass ratio of 1:5. With the addition of SiO₂, the phase transition temperature range of MCs increased from 34°C to 39°C, and the endothermic and exothermic latent heat decreased by 5.35 J/g and 10.07 J/g, respectively. The degradation rate of MCs was significantly slowed down at high temperature. The denim fabric coated with MCs revealed thermal regulation property. After absorbing heat, the MCs slowed down the rate of heat loss and extended the heat release time.

The phase transition temperature of the composite CM was wide, and the latent heat storage was reduced. The addition of SiO₂ particles can significantly slow down the rate of heat loss, but it further reduces the latent heat storage performance.

The method developed provided a simple and practical solution to improve the thermal regulation performance of fabrics.

The method of adjusting the phase transition temperature range of the composite CM is novel and many applications could be found in preparation of PCMs and thermal management.

Due to herbs and plants’ therapeutic properties and simplicity of availability in nature, humans have used them to treat a variety of maladies and diseases since ancient times. Later, as technology advanced, these plants and herbs gained significant relevance in some industries due to their suitable chemical composition, abundant availability and ease of access. Aegle marmelos is a species of plant that may be found in nature. Yet, little or very little literature was located on the coloration behavior of this plant’s leaves. This study aims to focus on the effect of different parameters on the extraction of colorant from Aegle marmelos leaves.

Some factors that affected on the extraction processes were examined and found to have significant impacts on the textile dyeing such as the initial dye concentration, extracted temperature, extracted bath pH and extracted time were all changed to see how they affected color extraction. The authors report a direct comparison between three heating methods, namely, microwave irradiation (MWI), ultrasonic waves (USW) and conventional heating (CH). The two kinetic models have been designed (pseudo-first and pseudo-second orders) in the context of these experiments to investigate the mechanism of the dyeing processes for fabrics under study. Also, the experimental data were analyzed according to the Langmuir and Freundlich isotherms.

From the result, it was discovered these characteristics were found to have a substantial effect on extraction efficiency. Temperature 90°C and 80°C when using CH and USW, respectively, while at 90% watt when using MWI, period 120 min when using CH as well as USW waves, while 40 min when using MWI, and pH 4, 5 and 10 for polyamide, wool and cotton, respectively, were the optimal extraction conditions. Also, the authors can say that wool gives a higher absorption than the other fabric. Additionally, MWI provided the best color strength (K/S) value, and homogeneity, at low temperatures reducing the energy and time consumed. The coloring follows the order: MWI > USW > CH. The adsorption isotherm of wool could be well fitted by Freundlich isotherm when applying CH and USW as a heating source, while it is well fitted by the Langmuir equation in the case of MWI. In the study, it was observed that the pseudo-first-order kinetic model fits better the experimental results of CH with a constant rate K₁ = −0.000171417 mg/g.min, while the pseudo-second-order kinetic model fits better the experimental results of absorption of both MWI (K2 = 38.14022572 mg/g.min) and USW (K₂ = 12.45343554 mg/g.min).

There is no research limitation for this work. Dye was extracted from Aegle marmelos leaves by applying three different heating sources (MWI, ultrasonic waves [USWW] and CH).

This work has practical applications for the textile industry. It is concluded that using Aegle marmelose leaves can be a possible alternative to extract dye from natural resource by applying new technology to save energy and time and can make the process greener.

Socially, it has a good impact on the ecosystem and global community because the extracted dye does not contain any carcinogenic materials.

The work is original and contains value-added products for the textile industry and other confederate fields.

The purpose of this study is to successfully apply ultrasonic waves for the quick extraction of flax seed gum from flaxseed hull or whole seed and compare it to the standard technique of extraction.

The effect of the heating source, extracted time, temperature and pH of extracted solution on the extraction was studied. The obtained gum is subsequently used for silk screen printing on cotton, linen and viscous fabrics. Rheological properties and viscosity of the printing paste were scrutinized in the current study to get a better insight into this important polysaccharide. The output of this effort aimed to specify the parameters of the processes for printing textiles to serve in women’s fashion clothes by applying innovated handmade combinations of Islamic art motives using a quick and affordable method. Seven designs are executed, and inspiring from them, seven fashion designs of ladies’ clothes were designed virtually by Clo 3D software.

The result recorded that the new gum has excellent printing properties. In addition, they have better rheological properties, viscosity, chromatic strength and fastness qualities, all of which could help them in commercial production.

Flaxseed and three different fabric types (Cotton, Linen and Viscous) were used.

Synthesis of a new biodegradable thickener from a natural resource, namely, flaxseed, by applying new technology to save time, water and energy.

Synthesis of eco-friendly biodegradable thickener and used in textile printing alternative to the synthetic thickener.

The textile sector is one of the sectors where competition is intense and requires the production of high-value-added products. This study aims to conduct patent analysis to find the technology status, recent trends, applications and technological evaluations of protective textile technologies in practice.

More than 36,840 patent documents related to protective textile technologies are available for researchers, patent examiners and patent researchers. Patent analysis is conducted to report the technology status, recent trends and applications of protective textile technologies. This analysis provides insights into the possible future directions of protective textile technologies in practice. Additionally, association rule mining (ARM) is performed to find the hidden patterns among protective textile technologies.

The development of protective textile technologies is revealed by the technology evaluation in this study. In addition, the sub-technology classes affecting protective textile technologies are examined using the cooperative patent classification (CPC) codes of the patent documents. Technology status and recent trends of protective textile technologies are provided in detail. The results of this study show that (1) protective textile technologies are constantly being developed, (2) the working areas of medical protective textiles are increasing, (3) there are frequent studies on fabric structures for saving lives within the framework of human needs and (4) there are four technology classes, namely A41D, Y10T, B32B and A62B impacting the other technology classes related to textile technologies such as D10B, Y10T, F41H, A62D, D04H, Y10S and D10B.

To have a competitive advantage in the marketplace, evaluation of textile technologies is critical in developing “functionalized” and “technologized” textile products. In particular, evaluating technologies in developing protective textile products is extremely important to meet customer demands and present competitive products in the market. Examining these patents for technology developers, decision-makers and policymakers is an urgent and necessary job. However, studies examining the development of protective textile technologies with patent analysis are very limited in the literature. To fill this gap, technology status, recent trends and applications of protective textile technologies are reported based on patent analysis and ARM in this study.

This paper aims to improve the adsorption capacity of sugarcane bagasse (SCB) as a low-cost, attractive and effective adsorbent for dye removal from wastewater.

SCB is a cellulosic material; it was chemically modified with compounds containing cationic groups. The adsorption efficiency of unmodified and modified SCB was investigated with anionic dyes by studying various factors that affect modified SCB and adsorption.

X-ray diffraction, FT-IR spectra and nitrogen content were used to confirm the effect of existence of quaternary ammonium groups on modified SCB. The morphological structure of the modified and unmodified SCB has been demonstrated using electronic scanning microscopy.

The modified SCB was chemically treated by Quat 188, which is commercially available in the solution of 3-chloro-2-hydroxypropyltrimethyl ammonium chloride.

Grafting cationic function groups on the surface of sugarcane by cationization treatment enhances its adsorption efficiency for anionic dyes.

The main value of this research was indicating a clear difference in the appearance of unmodified and modified SCB surfaces. Furthermore, it can be determined that the modified SCB absorbs more of the dyes.